29968-78-3
- Product Name：4-Nitrophenethylamine hydrochloride
- Molecular Formula：C8H11ClN2O2
- Purity：99%
- Molecular Weight：202.641
Product Details:
CasNo： 29968-78-3
Molecular Formula： C8H11ClN2O2
Appearance： light yellow crystal
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Factory Supply High Purity 4-Nitrophenethylamine hydrochloride,High Purity 99% 29968-78-3 Fast Delivery
- Molecular Formula:C8H11ClN2O2
- Molecular Weight:202.641
- Appearance/Colour:light yellow crystal
- Vapor Pressure:0.000737mmHg at 25°C
- Melting Point:200 °C (dec.)(lit.)
- Boiling Point:307.2 °C at 760 mmHg
- Flash Point:139.6 °C
- PSA：71.84000
- Density:1.206 g/cm3
- LogP:3.12150
4-Nitrophenethylamine hydrochloride(Cas 29968-78-3) Usage
|
Chemical Properties |
yellow to brown crystalline powder and chunks |
|
Uses |
4-Nitrophenethylamine hydrochloride was used in the synthesis of ortho-metalated primary phenethylamines complexes containing six-membered palladacycles and N-(4-nitrophenethyl)formamide. |
|
Preparation |
The preparation of 4-Nitrophenethylamine hydrochloride is as follows:Ten mL of 2M HCl was then added in a one-pot fashion, and, in all cases but threonine, the reaction vessel was heated to 190°Cover 5 min with stirring and then allowed to cool. In the case of the temperature-sensitive threonine, soxhlet extraction with toluene was performed at 80°C to remove R-carvone from the reaction mixture. The aqueous reaction mixture was washed three times with 25 mL of ether, and then water solvent was distilled off from the hydrochloride salt. The hydrochloride salt was transferred to a vacuum oven and dried overnight at 150 °C and 10 Torr. |
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29968-78-3 Relevant articles
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29968-78-3 Process route
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C18H22N2O2
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- 29968-78-3
2-(4-nitrophenyl)ethylamine monohydrochloride
| Conditions | Yield |
|---|---|
|
With hydrogenchloride; In propan-1-ol; at 190 ℃; for 0.0833333h; Microwave irradiation; Green chemistry;
|
74% |
-
- 6270-07-1
N-<2-(4-nitrophenyl)ethyl>acetamide
-
- 29968-78-3
2-(4-nitrophenyl)ethylamine monohydrochloride
| Conditions | Yield |
|---|---|
|
With hydrogenchloride; In ethanol; water; for 20h; pH=1; Reflux; Large scale;
|
84.7% |
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